Thin films of In2O3 by atomic layer deposition using In(acac)3
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Abstract
Thin films of indium oxide have been deposited using the atomic layer deposition (ALD) technique using In (acac)3 (acac = acetylacetonate, pentane-2,4-dione) and either H2O or 03 as precursors. Successful growth using In(acac)3 is contradictory to what has been reported previously in the literature [J.W. Elam, A.B.F. Martinson, M.J. Pellin, J.T. Hupp, Chem. Mater. 18 (2006) 3571.]. Investigation of the dependence of temperature on the deposition shows windows where the growth rates are relatively unaffected by temperature in the ranges 165-200 °C for In(acac)3 and H2O, 165-225 °C for In(acac)3 and 03. The growth rates obtained are of the order 20 pm/cycle for In(acac)3 and H2O,12 pm/cycle for In(acac)3.
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">Thin films of In<sub>2</sub>
O<sub>3</sub>
by atomic layer deposition using In(acac)<sub>3</sub>
</title>
<author><name sortKey="Nilsen, O" uniqKey="Nilsen O">O. Nilsen</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Centre for Materials Science and Nanotechnology (SMN), Department of Chemistry University of Oslo, P.B. 1033 Blindern</s1>
<s2>Oslo 0315</s2>
<s3>NOR</s3>
<sZ>1 aut.</sZ>
<sZ>5 aut.</sZ>
</inist:fA14>
<country>Norvège</country>
<wicri:noRegion>Oslo 0315</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Balasundaraprabhu, R" uniqKey="Balasundaraprabhu R">R. Balasundaraprabhu</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Centre for Materials Science and Nanotechnology (SMN), Department of Physics, University of Oslo, P.B. 1048, Blindem</s1>
<s2>Oslo 0316</s2>
<s3>NOR</s3>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>6 aut.</sZ>
</inist:fA14>
<country>Norvège</country>
<wicri:noRegion>Oslo 0316</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Monakhov, E V" uniqKey="Monakhov E">E. V. Monakhov</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Centre for Materials Science and Nanotechnology (SMN), Department of Physics, University of Oslo, P.B. 1048, Blindem</s1>
<s2>Oslo 0316</s2>
<s3>NOR</s3>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>6 aut.</sZ>
</inist:fA14>
<country>Norvège</country>
<wicri:noRegion>Oslo 0316</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Muthulcumarasamy, N" uniqKey="Muthulcumarasamy N">N. Muthulcumarasamy</name>
<affiliation wicri:level="1"><inist:fA14 i1="03"><s1>Department of Physics, Coimbatore Institute of Technology</s1>
<s2>Coimbatore</s2>
<s3>IND</s3>
<sZ>4 aut.</sZ>
</inist:fA14>
<country>Inde</country>
<wicri:noRegion>Coimbatore</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Fjellvag, H" uniqKey="Fjellvag H">H. Fjellvag</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Centre for Materials Science and Nanotechnology (SMN), Department of Chemistry University of Oslo, P.B. 1033 Blindern</s1>
<s2>Oslo 0315</s2>
<s3>NOR</s3>
<sZ>1 aut.</sZ>
<sZ>5 aut.</sZ>
</inist:fA14>
<country>Norvège</country>
<wicri:noRegion>Oslo 0315</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Svensson, B G" uniqKey="Svensson B">B. G. Svensson</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Centre for Materials Science and Nanotechnology (SMN), Department of Physics, University of Oslo, P.B. 1048, Blindem</s1>
<s2>Oslo 0316</s2>
<s3>NOR</s3>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>6 aut.</sZ>
</inist:fA14>
<country>Norvège</country>
<wicri:noRegion>Oslo 0316</wicri:noRegion>
</affiliation>
</author>
</titleStmt>
<publicationStmt><idno type="inist">09-0441229</idno>
<date when="2009">2009</date>
<idno type="stanalyst">PASCAL 09-0441229 INIST</idno>
<idno type="RBID">Pascal:09-0441229</idno>
<idno type="wicri:Area/Main/Corpus">004E83</idno>
<idno type="wicri:Area/Main/Repository">004908</idno>
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<seriesStmt><idno type="ISSN">0040-6090</idno>
<title level="j" type="abbreviated">Thin solid films</title>
<title level="j" type="main">Thin solid films</title>
</seriesStmt>
</fileDesc>
<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Atomic layer method</term>
<term>Crystal growth from vapors</term>
<term>Growth mechanism</term>
<term>Growth rate</term>
<term>Indium oxide</term>
<term>Precursor</term>
<term>Temperature dependence</term>
<term>Thin films</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Couche mince</term>
<term>Méthode couche atomique</term>
<term>Croissance cristalline en phase vapeur</term>
<term>Précurseur</term>
<term>Mécanisme croissance</term>
<term>Dépendance température</term>
<term>Taux croissance</term>
<term>Oxyde d'indium</term>
<term>In2O3</term>
<term>8115K</term>
<term>6855A</term>
</keywords>
</textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en">Thin films of indium oxide have been deposited using the atomic layer deposition (ALD) technique using In (acac)<sub>3</sub>
(acac = acetylacetonate, pentane-2,4-dione) and either H<sub>2</sub>
O or 0<sub>3</sub>
as precursors. Successful growth using In(acac)<sub>3</sub>
is contradictory to what has been reported previously in the literature [J.W. Elam, A.B.F. Martinson, M.J. Pellin, J.T. Hupp, Chem. Mater. 18 (2006) 3571.]. Investigation of the dependence of temperature on the deposition shows windows where the growth rates are relatively unaffected by temperature in the ranges 165-200 °C for In(acac)<sub>3</sub>
and H<sub>2</sub>
O, 165-225 °C for In(acac)<sub>3</sub>
and 0<sub>3</sub>
. The growth rates obtained are of the order 20 pm/cycle for In(acac)<sub>3</sub>
and H<sub>2</sub>
O,12 pm/cycle for In(acac)<sub>3</sub>
.</div>
</front>
</TEI>
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<fA08 i1="01" i2="1" l="ENG"><s1>Thin films of In<sub>2</sub>
O<sub>3</sub>
by atomic layer deposition using In(acac)<sub>3</sub>
</s1>
</fA08>
<fA09 i1="01" i2="1" l="ENG"><s1>Proceedings on the Sixth Symposium on Thin Films for Large Area Electronics</s1>
</fA09>
<fA11 i1="01" i2="1"><s1>NILSEN (O.)</s1>
</fA11>
<fA11 i1="02" i2="1"><s1>BALASUNDARAPRABHU (R.)</s1>
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<fA11 i1="03" i2="1"><s1>MONAKHOV (E. V.)</s1>
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<fA11 i1="04" i2="1"><s1>MUTHULCUMARASAMY (N.)</s1>
</fA11>
<fA11 i1="05" i2="1"><s1>FJELLVAG (H.)</s1>
</fA11>
<fA11 i1="06" i2="1"><s1>SVENSSON (B. G.)</s1>
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<fA12 i1="01" i2="1"><s1>SCHROPP (Ruud E.I.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="02" i2="1"><s1>ROCA I CABARROCAS (Pere)</s1>
<s9>ed.</s9>
</fA12>
<fA14 i1="01"><s1>Centre for Materials Science and Nanotechnology (SMN), Department of Chemistry University of Oslo, P.B. 1033 Blindern</s1>
<s2>Oslo 0315</s2>
<s3>NOR</s3>
<sZ>1 aut.</sZ>
<sZ>5 aut.</sZ>
</fA14>
<fA14 i1="02"><s1>Centre for Materials Science and Nanotechnology (SMN), Department of Physics, University of Oslo, P.B. 1048, Blindem</s1>
<s2>Oslo 0316</s2>
<s3>NOR</s3>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>6 aut.</sZ>
</fA14>
<fA14 i1="03"><s1>Department of Physics, Coimbatore Institute of Technology</s1>
<s2>Coimbatore</s2>
<s3>IND</s3>
<sZ>4 aut.</sZ>
</fA14>
<fA15 i1="01"><s1>Utrecht University, Faculty of Science, Department of Physics and Astronomy, Debye Institute for Nanomaterials Science, Section Nanophotonics, P.O. Box 80.000</s1>
<s2>3508 TA Utrecht</s2>
<s3>NLD</s3>
<sZ>1 aut.</sZ>
</fA15>
<fA15 i1="02"><s1>Laboratoire de Physique des Interfaces et des Couches Minces, Ecole Polytechnique</s1>
<s2>91128 Palaiseau</s2>
<s3>FRA</s3>
<sZ>2 aut.</sZ>
</fA15>
<fA20><s1>6320-6322</s1>
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<fA21><s1>2009</s1>
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<fA23 i1="01"><s0>ENG</s0>
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<fA43 i1="01"><s1>INIST</s1>
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<s1>© 2009 INIST-CNRS. All rights reserved.</s1>
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<fA45><s0>12 ref.</s0>
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<fA64 i1="01" i2="1"><s0>Thin solid films</s0>
</fA64>
<fA66 i1="01"><s0>CHE</s0>
</fA66>
<fC01 i1="01" l="ENG"><s0>Thin films of indium oxide have been deposited using the atomic layer deposition (ALD) technique using In (acac)<sub>3</sub>
(acac = acetylacetonate, pentane-2,4-dione) and either H<sub>2</sub>
O or 0<sub>3</sub>
as precursors. Successful growth using In(acac)<sub>3</sub>
is contradictory to what has been reported previously in the literature [J.W. Elam, A.B.F. Martinson, M.J. Pellin, J.T. Hupp, Chem. Mater. 18 (2006) 3571.]. Investigation of the dependence of temperature on the deposition shows windows where the growth rates are relatively unaffected by temperature in the ranges 165-200 °C for In(acac)<sub>3</sub>
and H<sub>2</sub>
O, 165-225 °C for In(acac)<sub>3</sub>
and 0<sub>3</sub>
. The growth rates obtained are of the order 20 pm/cycle for In(acac)<sub>3</sub>
and H<sub>2</sub>
O,12 pm/cycle for In(acac)<sub>3</sub>
.</s0>
</fC01>
<fC02 i1="01" i2="3"><s0>001B80A15K</s0>
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<fC02 i1="02" i2="3"><s0>001B80A15A</s0>
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<fC03 i1="01" i2="3" l="FRE"><s0>Couche mince</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="3" l="ENG"><s0>Thin films</s0>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="X" l="FRE"><s0>Méthode couche atomique</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="ENG"><s0>Atomic layer method</s0>
<s5>02</s5>
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<fC03 i1="02" i2="X" l="SPA"><s0>Método capa atómica</s0>
<s5>02</s5>
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<s5>03</s5>
</fC03>
<fC03 i1="03" i2="3" l="ENG"><s0>Crystal growth from vapors</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="3" l="FRE"><s0>Précurseur</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="3" l="ENG"><s0>Precursor</s0>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="X" l="FRE"><s0>Mécanisme croissance</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="ENG"><s0>Growth mechanism</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="SPA"><s0>Mecanismo crecimiento</s0>
<s5>05</s5>
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<s5>06</s5>
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<s5>06</s5>
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<s5>07</s5>
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<fC03 i1="07" i2="3" l="ENG"><s0>Growth rate</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE"><s0>Oxyde d'indium</s0>
<s5>15</s5>
</fC03>
<fC03 i1="08" i2="X" l="ENG"><s0>Indium oxide</s0>
<s5>15</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA"><s0>Indio óxido</s0>
<s5>15</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE"><s0>In2O3</s0>
<s4>INC</s4>
<s5>46</s5>
</fC03>
<fC03 i1="10" i2="3" l="FRE"><s0>8115K</s0>
<s4>INC</s4>
<s5>71</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE"><s0>6855A</s0>
<s4>INC</s4>
<s5>72</s5>
</fC03>
<fN21><s1>320</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
</fN44>
<fN82><s1>OTO</s1>
</fN82>
</pA>
<pR><fA30 i1="01" i2="1" l="ENG"><s1>E-MRS 2008 Spring Meeting. Symposium on Thin Films for Large Area Electronics.</s1>
<s3>Strasbourg FRA</s3>
<s4>2008-05-26</s4>
</fA30>
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